Quality and inspection

How to read a certificate of analysis.

A certificate of analysis states what a laboratory found in a sample. Whether it says anything useful about your container depends on which sample, which laboratory, which method and which date, and those four questions are the ones nobody asks.

Five checks.

Each takes a minute and together they catch most of what goes wrong with certificates in this trade. None of them requires technical knowledge.

  1. 01

    Which sample

    Does the certificate identify the lot that is shipping, by batch number or production date, and does that match your packing list? A certificate for a different batch is a certificate about somebody else's goods.

  2. 02

    Which laboratory

    In-house or independent, and accredited for what. A producer's own laboratory is not worthless and it has an interest. On anything where the number decides acceptance, independent is worth the cost.

  3. 03

    Which method

    Two laboratories using different methods produce different numbers on the same material, legitimately. If your specification names a method, the certificate has to use it or the comparison is meaningless.

  4. 04

    Which date

    Before or after the goods were packed. A result from material tested weeks before packing says nothing about moisture that was picked up since.

  5. 05

    Which properties

    Everything your specification asked for, or a subset. A certificate that reports four of your six properties has quietly not answered two questions.

What it does not prove.

That the rest of the container matches the sample. A certificate is analysis of a sample, and how representative that sample was depends on how it was taken. Sampling protocol is worth specifying on bulk agricultural goods.

That the goods are what they claim to be. Composition analysis on an essential oil establishes a profile. Species identification is a different test, and on products where substitution is the risk, that is the test you actually want.

That anything is safe. It reports numbers. Whether those numbers are acceptable is decided by your own market's limits and your own formulation, which is a question for your regulatory advisor rather than for the laboratory.

What to specify so the certificate is useful.

The properties, the limits, the method for each, and that the analysis is on the shipped lot. Then who takes the sample and how, because on bulk goods that is where representativeness is won or lost.

Where the value justifies it, split sampling: the producer's laboratory and an independent one on the same sample, with a retained portion sealed. It costs very little against a container and it converts a disagreement about results into a comparison.

Questions buyers ask.

Should I insist on an independent laboratory?

Where the number decides acceptance or price, yes. The cost is trivial against a container and the independence is the entire point. Where the analysis is routine confirmation of something visible, a producer's own result with a retained sample is often sufficient.

The certificate looks fine and the goods were not. Why?

Usually the sample. A certificate is honest about what was tested and says nothing about material it never saw. On bulk goods with variation, sampling protocol matters as much as the analysis, and it is the part almost nobody specifies.

Can a certificate be faked?

A PDF can be produced by anybody. That is one reason to name the laboratory in the specification and, where the value justifies it, to have the result confirmed with the laboratory directly. It is a five-minute check that is almost never done.

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